Transactions of Nonferrous Metals Society of China The Chinese Journal of Nonferrous Metals

您目前所在的位置:首頁 - 期刊簡介 - 詳細(xì)頁面

中國有色金屬學(xué)報

ZHONGGUO YOUSEJINSHU XUEBAO

第23卷    第4期    總第169期    2013年4月

[PDF全文下載]        

    

文章編號:1004-0609(2013)04-1079-07
K9和Si(100)基片上Be薄膜微觀組織、晶粒尺寸及表面粗糙度的演變規(guī)律
羅炳池1, 2,李  愷1, 2,李  佳1,譚秀蘭1, 2,周民杰1, 2,張吉強(qiáng)1,羅江山1, 2,吳衛(wèi)東1, 2,唐永建1

(1. 中國工程物理研究院 激光聚變研究中心,綿陽 621900;
2. 等離子體物理重點實驗室,綿陽 621900
)

摘 要: 采用真空蒸鍍法分別在K9和Si(100)基片上制備Be薄膜,在相同沉積速率下,K9基片上Be薄膜生長形態(tài)和Si基片上Be薄膜生長形態(tài)存在差異。但是兩者隨沉積速率增加具有相似的演變規(guī)律,即由等軸晶變化至纖維晶,再至粗大等軸晶。XRD和XPS分析結(jié)果表明:不同基片和蒸發(fā)溫度下制備的Be薄膜均主要由HCP結(jié)構(gòu)的α-Be相組成,且表面存在一定氧化;對于非晶K9基片,Be薄膜晶粒取向較單一,(101)始終為顯露晶面;而單晶Si(100)基片上Be晶粒取向多樣,在一定沉積速率下顯露特定晶面;相同沉積時間下K9和Si(100)基體上生長的Be薄膜粗糙度Rq變化趨勢十分相似,兩者隨Be薄膜沉積速率(v)增加先急劇增大后趨于平緩;以細(xì)小等軸晶生長的薄膜表面光潔度較高,而以纖維晶或粗大混晶生長的薄膜表面粗糙度較大。

 

關(guān)鍵字: Be薄膜;等軸晶;沉積速率;表面粗糙度

Evolution rule of microstructure, crystal grain size and surface roughness for Be films grown on K9 and Si(100) substrates
LUO Bing-chi1, 2, LI Kai1, 2, LI Jia1, TAN Xiu-lan1, 2, ZHOU Min-jie1, 2, ZHANG Ji-qiang1, LUO Jiang-shan1, 2, WU Wei-don

1. Research Center of Laser Fusion, China Academy of Engineering Physics, Mianyang 621900, China;
2. Science and Technology on Plsama Physics Laboratory, Mianyang 621900, China

Abstract:Be films grown on K9 and Si(100) substrates were fabricated by an evaporation deposition method. At the same deposition velocity, the growth morphology of Be films grown on the K9 substrate is different from that grown on the Si(100) substrate. Whereas, both of them have the similar evolution rule with the increase of deposition velocity, which changes from an equiaxed grain to a fiber grain, and then to a coarsening equiaxed grain. XRD and XPS analyses indicate that the Be films grown on different substrates at different deposition velocities consist mainly of HCP structure α-Be phase, and all of the Be film surface is oxidized. For the amorphous K9 substrate, the preferential growth orientation of Be film is always exposed to (101) crystal face. While, the grain orientation of the Si substrate is diversiform, a special crystal face can be shown at a certain deposition velocity. For the Be films grown on K9 substrate and Si(100) substrate, their variation trend of roughness Rq is similar at the same deposition time. Both of them increase sharply with the increase of deposition velocity, and then enhance slightly. The Be films with an equiaxed grain is very smooth, while the surface roughness of the fiber grain and coarsening mixed grain is very large.

 

Key words: Be films; equiaxed grain; deposition velocity; surface roughness

ISSN 1004-0609
CN 43-1238/TG
CODEN: ZYJXFK

ISSN 1003-6326
CN 43-1239/TG
CODEN: TNMCEW

主管:中國科學(xué)技術(shù)協(xié)會 主辦:中國有色金屬學(xué)會 承辦:中南大學(xué)
湘ICP備09001153號 版權(quán)所有:《中國有色金屬學(xué)報》編輯部
------------------------------------------------------------------------------------------
地 址:湖南省長沙市岳麓山中南大學(xué)內(nèi) 郵編:410083
電 話:0731-88876765,88877197,88830410   傳真:0731-88877197   電子郵箱:f_ysxb@163.com  
浏阳市| 思南县| 阜新市| 濉溪县| 怀安县| 广丰县| 陆川县| 合肥市| 鹤峰县| 土默特右旗| 中阳县| 易门县| 黑山县| 洪湖市| 筠连县| 乌兰县| 安远县| 宜宾市| 蓬安县| 雷州市| 资中县| 始兴县| 犍为县| 怀宁县| 宽甸| 阜城县| 基隆市| 英超| 革吉县| 鹤峰县| 汽车| 开江县| 稷山县| 三原县| 登封市| 扎鲁特旗| 布尔津县| 小金县| 朝阳市| 恩施市| 南投县|