(蘭州理工大學(xué) 省部共建有色金屬先進(jìn)加工與再利用國(guó)家重點(diǎn)實(shí)驗(yàn)室,蘭州 730050)
摘 要: 利用等通道轉(zhuǎn)角法(Equal channel angular pressing)對(duì)純銅進(jìn)行擠壓變形,研究變形過(guò)程中純銅組織演變,分析位錯(cuò)密度及其相應(yīng)力學(xué)性能變化規(guī)律,探討層錯(cuò)能對(duì)組織演變的影響機(jī)理。結(jié)果表明:退火后純銅在ECAP變形過(guò)程中由小角度晶界逐漸轉(zhuǎn)變?yōu)榇蠼嵌染Ы纾Я3叽缂?xì)化到5~10 μm;隨著擠壓道次的增加,純銅中位錯(cuò)密度顯著增大,1道次時(shí)位錯(cuò)密度為0.16×1014 m-2,6道次后位錯(cuò)密度達(dá)到最大值,為0.41×1014 m-2,之后位錯(cuò)重組和湮滅使得位錯(cuò)密度在一定程度上減小;材料強(qiáng)度明顯提高,塑性減小,退火后純銅的抗拉強(qiáng)度為220 MPa,伸長(zhǎng)率為53.5%,8道次后純銅的抗拉強(qiáng)度為444 MPa,伸長(zhǎng)率下降到22.1%;純銅拉伸斷口韌窩數(shù)量逐漸增多、變淺且分布均勻,斷裂方式整體表現(xiàn)為塑性斷裂。通過(guò)對(duì)組織演化和力學(xué)性能分析得出,純銅作為中等層錯(cuò)能材料,同時(shí)具有低層錯(cuò)能和高層錯(cuò)能金屬的一些變形特征。
關(guān)鍵字: 純銅;等通道轉(zhuǎn)角擠壓;位錯(cuò)密度;力學(xué)性能;層錯(cuò)能
(State Key Laboratory of Advanced Processing and Recycling of Nonferrous Metals,
Lanzhou University of Technology, Lanzhou 730050, China)
Abstract:The microstructure evolution, dislocation density and mechanical properties of pure copper via equal channel angular pressing were studied to investigate the effects of stack fault energy on the microstructure evolution. The results show that the grain size of annealed pure copper is refined into 5-10 μm, the small grain boundary turns into large ones, subsequently. The dislocation density is 0.16×1014 m-2 after 1 pass and reaches the maximum of 0.41×1014 m-2 after 6 passes, which increases remarkably with increasing the passes. While the recombination and annihilation of dislocations give rise to subsequent density decrease. The tensile strength of annealed copper is 220 MPa with elongation of 53.5%, while the tensile strength reaches 444 MPa and elongation reduces to 22.1% after 8 passes, which reveals that ECPA leads to the improvement of tensile strength and reduction of plasticity. The increased shallow dimple amounts and more uniform distribution of pure copper reveal its ductile fracture mechanism. The results of the microstructure evolution and mechanical property analysis show that, pure copper, as the middle stack fault energy metal material, possesses the characteristic of metal materials with high or low stack fault energy.
Key words: pure copper; ECAP; dislocation density; mechanical property; stacking fault energy


