Transactions of Nonferrous Metals Society of China The Chinese Journal of Nonferrous Metals

您目前所在的位置:首頁(yè) - 期刊簡(jiǎn)介 - 詳細(xì)頁(yè)面

中國(guó)有色金屬學(xué)報(bào)

ZHONGGUO YOUSEJINSHU XUEBAO

第18卷    第10期    總第115期    2008年10月

[PDF全文下載]        

    

文章編號(hào):1004-0609(2008)10-1858-06
超重力條件下電沉積金屬鎳的結(jié)構(gòu)與性能
劉 婷1, 2,郭占成1, 3,王 志1,王明涌1

(1. 中國(guó)科學(xué)院過程工程研究所 多相復(fù)雜系統(tǒng)國(guó)家重點(diǎn)實(shí)驗(yàn)室,北京 100190;
2. 中國(guó)科學(xué)院 研究生院,北京 100049;
3. 北京科技大學(xué) 循環(huán)與生態(tài)冶金教育部重點(diǎn)實(shí)驗(yàn)室,北京 100083
)

摘 要:

在超重力垂直于電極表面的情況下,研究超重力場(chǎng)對(duì)水溶液金屬電沉積鎳箔的組織結(jié)構(gòu)和性能的影響,利用原子力顯微鏡(AFM)和X射線衍射儀(XRD)對(duì)沉積鎳箔的表面形貌和晶體結(jié)構(gòu)進(jìn)行觀察。結(jié)果表明:超重力場(chǎng)下的鎳箔晶粒細(xì)化,表面更平整,當(dāng)重力系數(shù)為354時(shí),表面粗糙度由常重力下的20.9 nm降低到4.9 nm;并且隨著重力系數(shù)的增加,沉積鎳箔的晶體結(jié)構(gòu)從有擇優(yōu)取向結(jié)構(gòu)轉(zhuǎn)變?yōu)闊o特定的擇優(yōu)取向結(jié)構(gòu)。力學(xué)性能測(cè)試表明,當(dāng)重力系數(shù)為354時(shí),沉積鎳箔的硬度和抗拉強(qiáng)度分別達(dá)到HV 898和944 MPa,比常重力下分別提高了HV 604和646 MPa。

 

關(guān)鍵字: 鎳箔;超重力場(chǎng);重力系數(shù);電沉積;結(jié)構(gòu);性能

Structure and properties of electrochemically deposited nickel under high gravity field
LIU Ting1, 2, GUO Zhan-cheng1, 3, WANG Zhi1, WANG Ming-yong1

1. State Key Laboratory of Mutiphase Complex System, Institute of Process Engineering, Chinese Academy of Sciences, Beijing 100190, China;
2. Graduate University of Chinese Academy of Sciences, Beijing 100049, China;
3. Laboratory of Ecological and Recycle Metallurgy, University of Science and Technology Beijing, Beijing 100083, China

Abstract:In a high gravity field vertical to electrode surface, the effects of high gravity on the microstructure and properties of Ni film deposited electrochemically were investigated. With atomic force microscopy (AFM) and X-Ray diffraction. The results reveal that the surface structure of nickel film deposited under high gravity condition was more uniform and smoother compared with that in normal gravity condition; under G = 354, the roughness decreased sharply from 20.9 nm to 4.9 nm, and crystal grains diminished with the increasing of gravity coefficient. Furthermore, its crystal structure transforms from tropism to non-tropism with gravity coefficient. The hardness and tensile stress of nickel film are raised markedly to HV898 and 944 MPa when the gravity coefficient was up to 354 g, higher than those in normal gravity condition by HV604 and 646 MPa, respectively.

 

Key words: nickel film; high gravity field; gravity coefficient; electro-deposition; structure; property

ISSN 1004-0609
CN 43-1238/TG
CODEN: ZYJXFK

ISSN 1003-6326
CN 43-1239/TG
CODEN: TNMCEW

主管:中國(guó)科學(xué)技術(shù)協(xié)會(huì) 主辦:中國(guó)有色金屬學(xué)會(huì) 承辦:中南大學(xué)
湘ICP備09001153號(hào) 版權(quán)所有:《中國(guó)有色金屬學(xué)報(bào)》編輯部
------------------------------------------------------------------------------------------
地 址:湖南省長(zhǎng)沙市岳麓山中南大學(xué)內(nèi) 郵編:410083
電 話:0731-88876765,88877197,88830410   傳真:0731-88877197   電子郵箱:f_ysxb@163.com  
常山县| 德格县| 西盟| 海安县| 南部县| 新晃| 乌拉特后旗| 建昌县| 安丘市| 武隆县| 泸定县| 林州市| 富阳市| 海盐县| 青田县| 滨海县| 抚松县| 新乐市| 航空| 广西| 郴州市| 江安县| 潜江市| 汝州市| 新干县| 阿尔山市| 荥阳市| 胶州市| 沁水县| 日喀则市| 长沙市| 盐山县| 腾冲县| 浠水县| 灌云县| 安龙县| 衡南县| 乌恰县| 平南县| 龙岩市| 青龙|