Transactions of Nonferrous Metals Society of China The Chinese Journal of Nonferrous Metals

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中國有色金屬學(xué)報

ZHONGGUO YOUSEJINSHU XUEBAO

第18卷    第6期    總第111期    2008年6月

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文章編號:1004-0609(2008)06-1039-06
細(xì)晶鉬銅合金的制備
陳玉柏,范景蓮,劉  濤,成會朝,田家敏

(中南大學(xué) 粉末冶金國家重點實驗室,長沙 410083)

摘 要:

采用溶膠-噴霧干燥-煅燒-氫還原方法制取晶粒尺寸為17~50 nm的超細(xì)Mo-30Cu復(fù)合粉末,研究燒結(jié)溫度、時間和粉末中的氧含量對燒結(jié)致密化的影響,檢測合金的拉伸力學(xué)性能,分析合金的拉伸斷口形貌特征。結(jié)果表明:還原溫度對粉末形貌有很大的影響;在1 050~1 200 ℃燒結(jié)即可實現(xiàn)材料的快速致密化,在1 050 ℃燒結(jié)后保溫60 min時,合金的相對密度可達(dá)99%以上,并且晶粒細(xì)小,顯微組織分布均勻;合金的最大抗拉強(qiáng)度可達(dá)755 MPa,伸長率為6.41%。

 

關(guān)鍵字: Mo-Cu合金;超細(xì)粉末;力學(xué)性能;斷裂機(jī)制

Fabrication of fine-grained Mo-Cu alloy
CHEN Yu-bo, FAN Jing-lian, LIU Tao, CHENG Hui-chao, TIAN Jia-min

State Key Laboratory of Powder Metallurgy, Central South University, Changsha 410083, China

Abstract:Ultra-fine Mo-30Cu composite powders with grain size of 17−50 nm were fabricated by sol-spray drying, calcination and subsequent hydrogen reduction process. The results show that the influence of sintering temperature, time and the oxygen content in the powder on sintering densification were investigated. Meanwhile the tensile mechanical property of alloys was examined, and the tensile fracture surface features of the alloys were analysed. The results show that the reduction temperature has a great impact on powder morphology; the rapid densification can be realized in those green compacts, which are sintered in the temperature range of 1 050−1 200 ℃; when they are sintered at 1 050 ℃ for 60 min in H2 atmosphere, the relative density can achieve 99%, and their grains are fine, and the microstructures are homogeneous. The maximum tensile strength and elongation rate of the alloy are 755 MPa and 6.41%, respectively.

 

Key words: Mo-Cu alloy; ultra-fine powders; mechanical property; fracture mechanism

ISSN 1004-0609
CN 43-1238/TG
CODEN: ZYJXFK

ISSN 1003-6326
CN 43-1239/TG
CODEN: TNMCEW

主管:中國科學(xué)技術(shù)協(xié)會 主辦:中國有色金屬學(xué)會 承辦:中南大學(xué)
湘ICP備09001153號 版權(quán)所有:《中國有色金屬學(xué)報》編輯部
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