Transactions of Nonferrous Metals Society of China The Chinese Journal of Nonferrous Metals

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中國有色金屬學報

ZHONGGUO YOUSEJINSHU XUEBAO

第17卷    第7期    總第100期    2007年7月

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文章編號: 1004-0609(2007)07-1166-06
高硅鋁合金粉末的高溫空氣氧化預處理工藝
楊伏良,易丹青,劉 泓,張 偉

(中南大學 材料科學與工程學院,長沙 410083)

摘 要:

通過對鋁硅合金粉末采用高溫空氣氧化預處理,然后進行包套熱擠壓,制備了Al-12Si共晶及Al-30Si過共晶高硅鋁合金材料。利用氧分析儀、金相顯微鏡、掃描電鏡及透射電鏡等分析檢測設備,對預處理粉末的氧含量與組織及所制備材料組織進行分析比較。結果表明:鋁硅合金粉末氧含量隨氧化時間延長而逐漸增加,氧化速度隨氧化時間延長而下降;粉末顆粒表面氧含量明顯高于顆粒內部的;在相同氧化時間內,Al-30Si粉末氧含量的增加大于Al-12Si的,Al-30Si粉末的氧化速度更快;合金粉末經高溫空氣氧化預處理后,晶粒出現(xiàn)不同程度的長大,Al-12Si共晶合金的晶粒長大不明顯,而Al-30Si過共晶合金晶粒長大十分明顯。

 

關鍵字: 高硅鋁合金;電子封裝;高溫空氣預氧化

Pretreatment technology of high-silicon aluminum alloy powder in high
temperature atmosphere oxidation
YANG Fu-liang, YI Dan-qing, LIU Hong, ZHANG Wei

School of Materials Science and Engineering, Central South University, Changsha 410083, China

Abstract: In order to fabricate high-silicon aluminum alloy material, eutectic Al-12Si and hypereutectic Al-30Si alloy powders were pretreated in high temperature atmosphere oxidation, then they were canned and extruded into Al alloy materials. Oxygen analyzer, optical microscopy, scanning electron microscopy (SEM) and transmission electron microscopy (TEM), were used to study and compare the oxygen content and microstructure of pretreatment powders and the microstructure of materials. The results indicate that the oxygen content of the aluminum silicon alloy powders increases and the oxidation rate decreases with prolonging oxidation time. The oxygen content on powder surface is higher than that in inner particle. The oxygen content of Al-30Si powders is higher and the oxidation rate is quicker than that of Al-12Si powders in the same oxidation time. The crystal particles of alloy powders grow up in different degrees after pretreatment in high temperature atmosphere oxidation, the growth of size of Al-12Si eutectic alloy particles is not obvious, but that of Al-30Si hypereutectic alloy is very obvious.

 

Key words: high-silicon aluminum alloy; electronic packaging; high temperature atmosphere oxidation

ISSN 1004-0609
CN 43-1238/TG
CODEN: ZYJXFK

ISSN 1003-6326
CN 43-1239/TG
CODEN: TNMCEW

主管:中國科學技術協(xié)會 主辦:中國有色金屬學會 承辦:中南大學
湘ICP備09001153號 版權所有:《中國有色金屬學報》編輯部
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